N-Cbz-L-苯丙氨醛合成路线 （共 29 条）
反应条件
triethylamine in dichloromethane; dimethyl sulfoxide
反应条件
triethylamine; citric acid in dichloromethane; water; dimethyl sulfoxide
反应条件
dimethyl sulfoxide; triethylamine; citric acid in dichloromethane; water
反应条件
dimethyl sulfoxide; triethylamine; citric acid in dichloromethane
参考文献
US5461067 A1, ;
US 5461067 A
反应条件
diisobutylaluminium hydride in hexane; toluene T=-50°C;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 23, # 12 p. 3081 - 3087
反应条件
1: 19.1 g / Et3N / CH2Cl2 2: 70.3 percent / Et3SiH / 10 percent Pd/C / acetone / 20 °C View Scheme
参考文献
Synthesis, , # 8 p. 1121 - 1123
反应条件
1: NaHCO3 2: LiBH4 3: NaHCO3; NaOCl; NaBr / TEMPO / ethyl acetate; toluene; H2O / -5 °C View Scheme
参考文献
Heterocycles, , vol. 54, # 2 p. 581 - 584
反应条件
1: NaBH4; AcOH / methanol; dioxane 2: MnO2 / CHCl3 / 24 h / 20 °C View Scheme
参考文献
Synlett, , # 18 art. no. G24405ST, p. 2802 - 2804
反应条件
1: 87 percent / Et3N / tetrahydrofuran / 18 h / 20 °C 2: 76 percent / ethyldiisopropylamine; SO3/pyridine / CH2Cl2; dimethylsulfoxide / 0.5 h / cooling View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 11, # 24 p. 5449 - 5460
反应条件
1: aq. KHCO3 / ethyl acetate 2: iBu2AlH / hexane; toluene / -50 °C View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 23, # 12 p. 3081 - 3087
