1-(4-苄基氨基苯基)-乙酮合成路线 （共 8 条）
反应条件
potassium phosphate; copper(l) iodide; CVT-2537 in dimethyl sulfoxide
T=90°C; 24 h; Inert atmosphere;
参考文献
Zhang, Yu; Yang, Xinye; Yao, Qizheng; Ma, Dawei
Organic Letters, 2012 , vol. 14, # 12 p. 3056 - 3059
反应条件
potassium phosphate; ethylene glycol; copper(l) iodide in isopropyl alcohol
T=80°C; 5 h;
参考文献
Yang, Chu-Ting; Fu, Yao; Huang, Yao-Bing; Yi, Jun; Guo, Qing-Xiang; Liu, Lei
Angewandte Chemie, International Edition, 2009 , vol. 48, # 40 p. 7398 - 7401
Angewandte Chemie, 2009 , vol. 121, # 40 p. 7534 - 7537
反应条件
potassium hydroxide; biphenyl-2-yl-di-tert-butyl-phosphane; palladium diacetate in water; toluene
T=150°C; Buchwald-Hartwig amination; 0.5 h; microwave irradiation;
参考文献
Van Baelen, Gitte; Maes, Bert U.W.
Tetrahedron, 2008 , vol. 64, # 23 p. 5604 - 5619
反应条件
AlCl3, aluminium chloride in ethanol
T=70°C; 12 h; chemoselective reaction;
参考文献
Kumar, Vishal; Sharma, Sushila; Sharma, Upendra; Singh, Bikram; Kumar, Neeraj
Green Chemistry, 2012 , vol. 14, # 12 p. 3410 - 3414
反应条件
1: 4-nitrophenylacetoaldehyde With hydrogen in methanol; dichloromethane
T=20°C; P=760.051 Torr; 5.5 h;
2: benzaldehyde With hydrogen in methanol; dichloromethane
T=20°C; P=760.051 Torr; 2.5 h;
参考文献
Dell'Anna, Maria Michela; Mastrorilli, Piero; Rizzuti, Antonino; Leonelli, Cristina
Applied Catalysis A: General, 2011 , vol. 401, # 1-2 p. 134 - 140
反应条件
diborane in methanol
0.5 h; Ambient temperature;
参考文献
Nose, Atsuko; Kudo, Tadahiro
Chemical and Pharmaceutical Bulletin, 1986 , vol. 34, # 11 p. 4817 - 4820
反应条件
[RuIII(2,4-pentanedionato)3]; 1,2-bis-(diphenylphosphino)ethane in chlorobenzene
T=150°C; 48 h; Inert atmosphere;
参考文献
Liu, Yong; Chen, Wen; Feng, Chao; Deng, Guojun
Chemistry - An Asian Journal, 2011 , vol. 6, # 5 p. 1142 - 1146
反应条件
1: platinum(IV) oxide; hydrogen / methanol / 2 h / 20 °C
2: methanol / 2 h / 20 °C
3: hydrogen / methanol / 4 h / 20 °C
View Scheme
参考文献
Sreedhar, Bojja; Rawat, Vikas S.
Synthetic Communications, 2012 , vol. 42, # 17 p. 2490 - 2502
