反应条件
1.1: sodium tetrahydroborate / tetrahydrofuran / 0.25 h / 65 °C
1.2: 0.25 h / 65 °C
2.1: sodium chloride; methanesulfonyl chloride; triethylamine; 4-(N,N-dimethlyamino)pyridine / dichloromethane
View Scheme
参考文献
Bantreil, Xavier; Kanfar, Nasreddine; Gehin, Nicolas; Golliard, Ethan; Ohlmann, Pauline; Martinez, Jean; Lamaty, Frederic
Tetrahedron, 2014 , vol. 70, # 34 p. 5093 - 5099
