3.3-二甲基-4.6,6-三氯己烯[5]酸乙酯合成路线 （共 12 条）
参考文献
Kuraray Co., Ltd.
Patent: US4113968 A1, 1978 ;
反应条件
pyrrolidine in toluene
T=100 - 110°C; 4 h;
参考文献
Matsui, Kiyohide; Negishi, Akira; Takahatake, Yuriko; Sugimoto, Kikuo; Fujimoto, Tamotsu; et al.
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, # 1 p. 221 - 228
反应条件
in bis(2-methoxyethyl)ether (diglyme); diethylene glycol dimethyl ether
参考文献
Sagami Chemical Research Center
Patent: US4214097 A1, 1980 ;
参考文献
Sagami Chemical Research Center
Patent: US4214097 A1, 1980 ;
反应条件
hydrogenchloride in ethanol; water
参考文献
Kuraray Co., Ltd.
Patent: US4458090 A1, 1984 ;
反应条件
in xylene
T=130°C; 5 h;
参考文献
Matsui, Kiyohide; Negishi, Akira; Takahatake, Yuriko; Sugimoto, Kikuo; Fujimoto, Tamotsu; et al.
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, # 1 p. 221 - 228
参考文献
Kuraray Co., Ltd.
Patent: US4458090 A1, 1984 ;
反应条件
toluene-4-sulfonic acid
参考文献
Kuraray Co., Ltd.
Patent: US4113968 A1, 1978 ;
反应条件
1: 86 percent / BPO / 20 h / 80 °C
2: 87 percent / pyrrolidine / toluene / 4 h / 100 - 110 °C
View Scheme
参考文献
Matsui, Kiyohide; Negishi, Akira; Takahatake, Yuriko; Sugimoto, Kikuo; Fujimoto, Tamotsu; et al.
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, # 1 p. 221 - 228
反应条件
1: 85 percent / piperidine / benzene / 5 h / Ambient temperature
2: 90 percent / xylene / 5 h / 130 °C
View Scheme
参考文献
Matsui, Kiyohide; Negishi, Akira; Takahatake, Yuriko; Sugimoto, Kikuo; Fujimoto, Tamotsu; et al.
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, # 1 p. 221 - 228
