反应条件
1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 °C 1.2: 20 °C 2.1: lithium aluminium tetrahydride / diethyl ether / 0 °C 3.1: 4-(N,N-dimethlyamino)pyridine; triethylamine / dichloromethane / 0 °C 3.2: 20 °C 4.1: acetic acid / 20 °C 5.1: sodium periodate / methanol; water 6.1: sodium dihydrogenphosphate; sodium chlorite / methanol; dichloromethane; water / 20 °C 7.1: potassium carbonate / methanol / 20 °C 8.1: palladium 10 on activated carbon; hydrogen / methanol View Scheme
参考文献
Synthesis, , vol. 44, # 7 art. no. SS-2011-Z1183-OP, p. 1102 - 1108
