4,N-二甲基-n-苯基苯磺酰胺合成路线 (共 37 条)
参考文献
Beringer et al.
Journal of the American Chemical Society, 1953 , vol. 75, p. 2705,2707
Journal of the American Chemical Society, 1959 , vol. 81, p. 342,346
参考文献
Klammann et al.
Monatshefte fuer Chemie, 1952 , vol. 83, p. 870,872,876
参考文献
Arndt; Martius
Justus Liebigs Annalen der Chemie, 1932 , vol. 499, p. 228,283
反应条件
sodium hydroxide; water
versetzt die klare Loesung mit 10 ccm Dimethylsulfat;
参考文献
Ullmann
Justus Liebigs Annalen der Chemie, 1903 , vol. 327, p. 110
参考文献
Michler; Meyer,K.
Chemische Berichte, 1879 , vol. 12, p. 1792
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Bergel; Doering
Chemische Berichte, 1928 , vol. 61, p. 844
参考文献
Simonow
Zhurnal Obshchei Khimii, 1952 , vol. 22, p. 2006,2009; engl. Ausg. S. 2059, 2061
参考文献
Gloede,J.; Costisella,B.
Journal fuer Praktische Chemie (Leipzig), 1971 , vol. 313, p. 277 - 286
反应条件
T=150°C; decomposition;
参考文献
Challis, Brian C.; Iley, James N.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1985 , p. 699 - 704
反应条件
anschl. mit Dimethylsulfat;
参考文献
Ullmann
Justus Liebigs Annalen der Chemie, 1903 , vol. 327, p. 110
反应条件
1: With potassium salt of diphenylphosphine anion in tetrahydrofuran
T=-78°C; 2 h; Inert atmosphere;
2: With hydrogenchloride in tetrahydrofuran; water
T=20°C; 0.5 h; Inert atmosphere;
参考文献
Yoshida, Suguru; Igawa, Kazunobu; Tomooka, Katsuhiko
Journal of the American Chemical Society, 2012 , vol. 134, # 47 p. 19358 - 19361