N-对甲苯基-对甲苯磺胺合成路线 （共 64 条）
反应条件
1: [bis(acetoxy)iodo]benzene / 0.08 h / 25 °C / |Schlenk technique; |Inert atmosphere
2: bismuth trifluoromethanesulphonate / methanol / 25 °C / |Schlenk technique; |Inert atmosphere
3: zinc; trifluoroacetic acid / methanol / 25 °C / |Schlenk technique; |Inert atmosphere
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参考文献
Zhang, Li; Wang, Weibin; Fan, Renhua
Organic Letters, 2013 , vol. 15, # 8 p. 2018 - 2021
参考文献
Bell
Journal of the Chemical Society, 1955 , p. 2376,2379
反应条件
1: [bis(acetoxy)iodo]benzene / 0.08 h / 25 °C / |Schlenk technique; |Inert atmosphere
2: bismuth trifluoromethanesulphonate / methanol / 25 °C / |Schlenk technique; |Inert atmosphere
3: zinc; trifluoroacetic acid / methanol / 25 °C / |Schlenk technique; |Inert atmosphere
4: palladium diacetate; tri-cyclo-hexyl-phosphine; potassium carbonate; silver carbonate / N,N-dimethyl acetamide / 130 °C / |Schlenk technique; |Inert atmosphere
View Scheme
参考文献
Zhang, Li; Wang, Weibin; Fan, Renhua
Organic Letters, 2013 , vol. 15, # 8 p. 2018 - 2021
反应条件
1: glacial acetic acid; nitric acid / 70 °C
2: concentrated sulfuric acid
View Scheme
参考文献
Reverdin; de Luc
Chemische Berichte, 1910 , vol. 43, p. 3462
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1910 , vol. 151, p. 985
