N-(2-甲基-6-硝基苯基)-乙酰胺合成路线 (共 33 条)
反应条件
Bi(NO3)3·5H2O in dichloromethane T=23°C; regioselective reaction;
参考文献
Lu, Yang; Li, Yaming; Zhang, Rong; Jin, Kun; Duan, Chunying
Tetrahedron, 2013 , vol. 69, # 45 p. 9422 - 9427
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 30, p. 141 - 149
反应条件
nitric acid; acetic anhydride in ice-water
参考文献
Takasago International Corporation
Patent: US5021593 A1, 1991 ;
反应条件
tris(dibenzylideneacetone)dipalladium (0); caesium carbonate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in 1,4-dioxane T=100°C; Arylation; 16 h;
参考文献
Yin, Jingjun; Buchwald, Stephen L.
Organic Letters, 2000 , vol. 2, # 8 p. 1101 - 1104
反应条件
hydrogenchloride in acetic acid 1.5 h; Ambient temperature;
参考文献
Tanaka, Kenjiro; Shimazaki, Michiko; Murakami, Yasuoki
Chemical & Pharmaceutical Bulletin, 1982 , vol. 30, # 8 p. 2714 - 2722
反应条件
nitrogen(IV) oxide; ozone in chloroform 2 h; < 0 deg C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 32, # 45 p. 6591 - 6594
反应条件
1: 83.7 percent / 12.5 h / 120 °C 2: 85 percent / cc HCl / acetic acid / 1.5 h / Ambient temperature View Scheme
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 30, # 8 p. 2714 - 2722
反应条件
2: NO2, O3, O2 / CHCl3 / 2 h / 0 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 4 p. 339 - 344
参考文献
Journal of the Chemical Society, , vol. 117, p. 775
反应条件
Product distribution;
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2>102, p. 184