反应条件
1: 94 percent / LiCl, sodium borohydride, EtOH / tetrahydrofuran / 1) 0 deg C, 1 h, 2) r.t., 19.5 h
2: 95 percent / sulfur trioxide-pyridine complex, DMSO, Et3N / CH2Cl2 / 0.17 h / 10 - 20 °C
3: 61 percent / 0.4 M cerium chloride / methanol / 67 h / 40 - 45 °C
4: 10percent HCl / methanol / 1 h / Ambient temperature
5: diethyl phosphorocyanidate, triethylamine / tetrahydrofuran / 1) 0 deg C, 1 h, 2) r.t., 40 min
7: 80 percent / H2 / 5percent Pd-C / ethanol / 1 h / Ambient temperature
View Scheme
参考文献
Mori, Shigehiro; Ohno, Tomoyasu; Harada, Hiroshi; Aoyama, Toyohiko; Shioiri, Takayuki
Tetrahedron, 1991 , vol. 47, # 27 p. 5051 - 5070
