反应条件
1: triethylamine / methanol; dichloromethane / 2 h / 20 °C
2: 1,8-diazabicyclo[5.4.0]undec-7-ene; trichloromonobromomethane / dichloromethane / 0 - 4 °C / |Inert atmosphere
3: hydrogen; palladium 10 on activated carbon / ethanol / 72 h / 20 °C
View Scheme
参考文献
Popsavin, Mirjana; Kojic, Vesna; Spaic, Sasa; Svircev, Milos; Bogdanovic, Gordana; Jakimov, Dimitar; Aleksic, Lidija; Popsavin, Velimir
Tetrahedron, 2014 , vol. 70, # 14 p. 2343 - 2350
