1-乙氧基-3-三氟甲基-1,3-丁二烯合成路线 （共 52 条）
反应条件
in benzene T=120°C; 6 h;
参考文献
Gerus, I. I.; Vdovenko, S. I.; Gorbunova, M. G.; Kukhar', V. P.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1991 , vol. 27, # 4 p. 398 - 406
Khimiya Geterotsiklicheskikh Soedinenii, 1991 , # 4 p. 502 - 511
反应条件
in methanol 4 h; Heating;
参考文献
Schlosser, Manfred; Volle, Jean-Noel; Leroux, Frederic; Schenk, Kurt
European Journal of Organic Chemistry, 2002 , # 17 p. 2913 - 2920
反应条件
in methanol T=55°C; 20 h; Cooling with ice; Overall yield = 63 percent; Overall yield = 153 g;
参考文献
SOLVAY SA; BRAUN, Max Josef; FISCHER, Reiner
Patent: WO2013/167586 A1, 2013 ;
Location in patent: Page/Page column 10 ;
反应条件
in ethanol 2 h; Heating;
参考文献
Journal of Heterocyclic Chemistry, , vol. 39, # 5 p. 1025 - 1027
反应条件
in dichloromethane 2 h; Heating;
参考文献
Journal of Heterocyclic Chemistry, , vol. 40, # 6 p. 1087 - 1089
反应条件
in dichloromethane T=20°C; 2 h;
参考文献
Gerus, I. I.; Gorbunova, M. G.; Vdovenko, S. I.; Yagupol'skii, Yu. L.; Kukhar', V. P.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 9.1 p. 1623 - 1628
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 9 p. 1877 - 1883
反应条件
pyridine in water 36 h; Heating;
参考文献
Madruga, Claudia da C.; Clerici, Edflia; Martins, Marcos A. P.; Zanatta, Nilo
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 3 p. 735 - 738
反应条件
in water; acetonitrile Ambient temperature;
参考文献
Hojo, Masaru; Masuda, Ryoichi; Okada, Etsuji; Sakaguchi, Syuhei; Narumiya, Hitoshi; Morimoto, Katsushi
Tetrahedron Letters, 1989 , vol. 30, # 45 p. 6173 - 6176
反应条件
in ethanol T=20 - 80°C; Cycloaddition; 24 h;
参考文献
Chu, Qianli; Wang, Yanli; Zhu, Shizheng
Synthetic Communications, 2000 , vol. 30, # 4 p. 677 - 687
反应条件
hydrazine monohydrochloride in methanol T=15°C; Inert atmosphereRefluxIndustry scale;
参考文献
SOLVAY SA; BRAUN, Max
Patent: WO2010/37688 A1, 2010 ;
Location in patent: Page/Page column 8 ;
