反应条件
1: acetylacetone With N,N,N',N',N'',N''-hexamethylphosphoric triamide; sodium hydride in tetrahydrofuran
T=0°C; 0.333333 h; Inert atmosphere;
2: With n-butyllithium in tetrahydrofuran; hexane
0.333333 h; Inert atmosphere;
3: 1-(Chloromethyl)-4-vinylbenzene in tetrahydrofuran; hexane
T=20°C; 0.333333 h; Inert atmosphere;
参考文献
Thesen, Manuel W.; Krueger, Hartmut; Janietz, Silvia; Wedel, Armin; Graf, Marion
Journal of Polymer Science, Part A: Polymer Chemistry, 2010 , vol. 48, # 2 p. 389 - 402