phosphate buffer T=25°C; 0.5 h; var. buffer systems; var. aldehydes; also in the presence of ethanol; Mechanism;
参考文献
Huang, Tzou-Chi; Huang, Lee-Zen; Ho, Chi-Tang
Journal of Agricultural and Food Chemistry, 1998 , vol. 46, # 1 p. 224 - 227
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反应条件
potassium acetate in methanol; water byproducts: NH3; addn. of a soln. of 2-aminoethanethiol to a suspension of the Cu compd. in MeOH, addn. of an aqueous soln. of CH3COOK and stirring under reflux for 2 h; concn. to its half vol., cooling to 0°C yields the Cu complex, filtn., washing with MeOH and drying over P4O10; elem. anal.;
参考文献
Patel, B. V.; Desai, Kalpana; Thaker, B. T.
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 1989 , vol. 19, p. 391 - 412
Barnett, D.Jonathan; Rios, Ana; Williams, D. Lyn H.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1995 , # 7 p. 1279 - 1282