potassium hydroxide in water; tert-butyl alcohol
T=40°C; 4 h; electrolysis at a Ni(OH)2 anode and a steel cathode, current - 2 A, cell voltage - 2.0 V;
参考文献
Feldhues, U.; Schaefer, H. J.
Synthesis, 1982 , # 2 p. 145 - 146
1: 95 percent / Et3N / methanol / 18 h / 20 °C
2: 89 percent / EDC / dimethylformamide / 18 h / 20 °C
View Scheme
参考文献
McKeen, Catherine M.; Brown, Lynda J.; Nicol, Jamie T.G.; Mellor, John M.; Brown, Tom
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 13 p. 2267 - 2275
