in chloroform-d1 (red light conditions); a NMR tube containing the Mo-compd., PhSH and CDCl3 is prepared under N2, and then frozen, evacuated and sealed. Sample is heated at 60°C in a water bath.; monitored by NMR;
in chloroform; water aq. HCl was added to soln. of the complex in CHCl3 and react. mixt. wasstirred for 3 h; soln. was dried over MgSO4, volatiles were distilled off under vac., n-pentane was added;
