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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
乙酰胺
合成路线
（共 1192 条）
60-35-5
乙酰胺
+
79099-07-3
N-叔丁氧羰基-4-哌啶酮
→
反应条件
365996-05-0
2-氨基-6,7-二氢噻唑并[5,4-c]吡啶-5(4H)-甲酸叔丁酯
反应条件
1: tert-butyl 4-oxo-piperidine-1-carboxylate With pyrrolidine; toluene-4-sulfonic acid in cyclohexane 5 h; Heating / reflux; 2: acetamide With sulfur in methanol T=4°C; 2 h; Cooling with ice;
参考文献
BOEHRINGER INGELHEIM INTERNATIONAL GMBH; BOEHRINGER INGELHEIM PHARMA GMBH and CO. KG
Patent: WO2008/86047 A1, 2008 ;
Location in patent: Page/Page column 127-128 ;
WO 2008/086047 A1
60-35-5
乙酰胺
+
1338460-51-7
→
反应条件
95-20-5
2-甲基吲哚
反应条件
palladium diacetate; caesium carbonate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in 1,4-dioxane T=100°C; 19 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 76, # 21 p. 9060 - 9067
60-35-5
乙酰胺
+
109-67-1
正戊烯
+
201230-82-2
→
反应条件
123-15-9
2-甲基戊醛
+
757959-95-8
+
1430826-26-8
反应条件
Rh(acac)(CO)2; hydrogen; toluene-4-sulfonic acid; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in methanol; diethylene glycol dimethyl ether T=100°C; P=37503.8 Torr; 8 h; Inert atmosphereSchlenk technique; Reagent/catalystSolvent; chemoselective reaction;
参考文献
ChemSusChem, , vol. 6, # 9 p. 1759 - 1773
60-35-5
乙酰胺
+
109-67-1
正戊烯
+
201230-82-2
→
反应条件
105-30-6
+
66-25-1
+
111-27-3
反应条件
Rh(acac)(CO)2; hydrogen; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in diethylene glycol dimethyl ether T=100°C; P=37503.8 Torr; 8 h; Inert atmosphereSchlenk technique; Catalytic behavior; Reagent/catalystSolvent; chemoselective reaction;
参考文献
ChemSusChem, , vol. 6, # 9 p. 1759 - 1773
60-35-5
乙酰胺
+
109-67-1
正戊烯
+
201230-82-2
→
反应条件
757959-95-8
+
1430826-26-8
反应条件
Rh(acac)(CO)2; hydrogen; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in diethylene glycol dimethyl ether T=100°C; P=37503.8 Torr; 4 h; Inert atmosphereSchlenk technique; Catalytic behavior; Reagent/catalystSolvent; chemoselective reaction;
参考文献
ChemSusChem, , vol. 6, # 9 p. 1759 - 1773
60-35-5
乙酰胺
+
109-67-1
正戊烯
+
201230-82-2
→
反应条件
7501-79-3
+
757959-95-8
+
1430826-26-8
反应条件
Rh(acac)(CO)2; hydrogen; toluene-4-sulfonic acid; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in diethylene glycol dimethyl ether T=100°C; P=37503.8 Torr; 4 h; Inert atmosphereSchlenk technique; Catalytic behavior; Reagent/catalystSolvent; chemoselective reaction;
参考文献
ChemSusChem, , vol. 6, # 9 p. 1759 - 1773
60-35-5
乙酰胺
+
109-67-1
正戊烯
+
201230-82-2
→
反应条件
123-15-9
2-甲基戊醛
+
7501-79-3
+
757959-95-8
+
1430826-26-8
反应条件
Rh(acac)(CO)2; hydrogen; toluene-4-sulfonic acid; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in diethylene glycol dimethyl ether T=100°C; P=37503.8 Torr; 4 h; Inert atmosphereSchlenk technique; Catalytic behavior; Reagent/catalystSolvent; chemoselective reaction;
参考文献
ChemSusChem, , vol. 6, # 9 p. 1759 - 1773
60-35-5
乙酰胺
+
109-67-1
正戊烯
+
201230-82-2
→
反应条件
105-30-6
+
7501-79-3
+
757959-95-8
+
1430826-26-8
反应条件
Rh(acac)(CO)2; hydrogen; toluene-4-sulfonic acid; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in diethylene glycol dimethyl ether T=100°C; P=37503.8 Torr; 8 h; Inert atmosphereSchlenk technique; Catalytic behavior; Reagent/catalystSolvent; chemoselective reaction;
参考文献
ChemSusChem, , vol. 6, # 9 p. 1759 - 1773
60-35-5
乙酰胺
→
反应条件
75-04-7
+
109-89-7
+
121-44-8
反应条件
ammonia; hydrogen; Leuna 1970T T=250°C; P=7500.75 Torr;
参考文献
US2006/287556 A1, ;
Page/Page column 5 ;
60-35-5
乙酰胺
+
75-44-5
→
反应条件
75-36-5
+
75-05-8
反应条件
T=50°C;
参考文献
Schmidt,E.
Journal fuer Praktische Chemie (Leipzig), 1872 , vol. <2>5, p. 63
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