2-溴-2-甲基丙酸乙酯合成路线 (共 239 条)
反应条件
tetra-n-butylammonium tetrafluoroborate; zinc dibromide; zinc in acetonitrile Ambient temperature;
参考文献
Rollin, Y.; Gebehenne, C.; Derien, S.; Dunach, E.; Perichon, J.
Journal of Organometallic Chemistry, 1993 , vol. 461, # 1-2 p. 9 - 14
反应条件
mercury dichloride; zinc in diethyl ether; benzene
参考文献
Lapkin,I.I.; Fotin,V.V.
Journal of Organic Chemistry USSR (English Translation), 1975 , vol. 11, p. 2360 - 2362
Zhurnal Organicheskoi Khimii, 1975 , vol. 11, # 11 p. 2319 - 2322
参考文献
Lapin,H.; Horeau,A.
Gazzetta Chimica Italiana, 1963 , vol. 93, p. 451 - 454
参考文献
Bloom; Hauser
Journal of the American Chemical Society, 1944 , vol. 66, p. 153
反应条件
2,4,6-trimethyl-pyridine; 2,2'-azo-bisisobutyronitrile in benzene 3 h; Heating;
参考文献
Cai, Yudong; Roberts, Brian P.; Tocher, Derek A.; Barnett, Sarah A.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 17 p. 2517 - 2529
反应条件
zinc in methyl acetate
参考文献
Bowman, Mark P.; Senet, Jean-Pierre G.; Malfroot, Thierry; Olofson, R. A.
Journal of Organic Chemistry, 1990 , vol. 55, # 24 p. 5982 - 5986
反应条件
potassium carbonate in N,N-dimethyl-formamide T=70°C; 25 h;
参考文献
ADVINUS THERAPEUTICS PRIVATE LIMITED
Patent: WO2008/104994 A2, 2008 ;
Location in patent: Page/Page column 32-33 ;
WO 2008/104994 A2
反应条件
zinc durch Zersetzung des Reaktionsprodukts mit Wasser;
参考文献
Mazet,M.; Desmaison-Brut,M.
Bulletin de la Societe Chimique de France, 1971 , p. 2656 - 2662
反应条件
ethanol anschliessend Erwaermen mit wss. Natronlauge;
参考文献
Fawcett et al.
Annals of Applied Biology, 1955 , vol. 43, p. 342,343, 344
Proceedings of the Royal Society of London, Series B: Biological Sciences, 1959 , vol. 150, p. 95,96, 100
反应条件
indium in N,N-dimethyl-formamide 2 h; Heating; Yield given. Yields of byproduct given;
参考文献
Schick, Hans; Ludwig, Ralf; Schwarz, Karl-Heinz; Kleiner, Katharina; Kunath, Annamarie
Journal of Organic Chemistry, 1994 , vol. 59, p. 3161 - 3164