2-溴-2-甲基丙酸乙酯合成路线 (共 239 条)
参考文献
Zerk, Timothy J.; Bernhardt, Paul V.
Dalton Transactions, 2013 , vol. 42, # 32 p. 11683 - 11694
反应条件
decacarbonyldimanganese (2) in tetrahydrofuran 0.5 h; Irradiationor CDCl3; Further byproducts given;
参考文献
Masters, Andrew P.; Sorensen, Ted S.
Canadian Journal of Chemistry, 1990 , vol. 68, # 3 p. 492 - 501
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; lithium diisopropyl amide THF, hexane, -78 deg C; Yield given. Multistep reaction;
参考文献
Petragnani, Nicola; Yonashiro, Massami
Synthesis, 1980 , # 9 p. 710 - 713
反应条件
in tetrahydrofuran (N2 or Ar); solution is allowed to stand for 5 h; determination by NMR and MS fragmentation;
参考文献
Masters, Andrew P.; Sorensen, Ted S.
Canadian Journal of Chemistry, 1990 , vol. 68, # 3 p. 492 - 501
反应条件
in tetrahydrofuran (N2 or Ar); solution is allowed to stand for 5 h; determination by NMR and MS fragmentation;
参考文献
Masters, Andrew P.; Sorensen, Ted S.
Canadian Journal of Chemistry, 1990 , vol. 68, # 3 p. 492 - 501
反应条件
in tetrahydrofuran Irradiation (UV/VIS); (N2 or Ar); 250-W sun lamp, 3 h; colorless solution is filtered, (1)H-NMR;
参考文献
Masters, Andrew P.; Sorensen, Ted S.
Canadian Journal of Chemistry, 1990 , vol. 68, # 3 p. 492 - 501
反应条件
zinc; benzene Das Aethylester entsteht. Man verseift den Aethylester mit alkoh.Kalilauge;
参考文献
Blaise; Courtot
Bulletin de la Societe Chimique de France, 1906 , vol. <3> 35, p. 367,370
参考文献
Blaise; Courtot
Bulletin de la Societe Chimique de France, 1906 , vol. <3> 35, p. 367,370
反应条件
sodium methylate in methanol; toluene
参考文献
Ito, Mitsuru; Okui, Hideshi; Nakagawa, Harumi; Mio, Shigeru; Iwasaki, Toshiaki; Iwabuchi, Jun
Heterocycles, 2002 , vol. 57, # 5 p. 881 - 894
参考文献
Iro, Mitsuru; Okui, Hideshi; Nakagawa, Harumi; Mio, Shigeru; Kinoshita, Ayako; Obayashi, Takashi; Miura, Takako; Nagai, Junko; Yokoi, Shinji; Ichinose, Reiji; Tanaka, Keiji; et al.
Bioscience, Biotechnology, and Biochemistry, 2002 , vol. 66, # 11 p. 2406 - 2414