2-溴-2-甲基丙酸乙酯合成路线 （共 239 条）
反应条件
potassium tert-butylate in tetrahydrofuran T=60°C; 2 h; Inert atmosphere;
参考文献
Oh, Lynette M.; Wang, Huan; Shilcrat, Susan C.; Hermann, Robert E.; Patience, Daniel B.; Spoors, P. Grant; Sisko, Joseph
Organic Process Research and Development, 2007 , vol. 11, # 6 p. 1032 - 1042
反应条件
{bis(triphenylphosphine)nitrogen}{manganese(carbonyl)5} in tetrahydrofuran 5 h;
参考文献
Canadian Journal of Chemistry, , vol. 68, # 3 p. 492 - 501
参考文献
Blaise; Courtot
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1905 , vol. 140, p. 371
Full Text Show Details
Blaise; Luttringer
Bulletin de la Societe Chimique de France, 1905 , vol. <3> 33, p. 1101
Full Text Show Details
v. Auwers; Koenig
Justus Liebigs Annalen der Chemie, 1932 , vol. 496, p. 38,42
反应条件
in tetrahydrofuran (N2 or Ar); solution is allowed to stand for 5 h; determination by NMR and MS fragmentation;
参考文献
Canadian Journal of Chemistry, , vol. 68, # 3 p. 492 - 501
反应条件
in tetrahydrofuran (N2 or Ar); solution is allowed to stand for 5 h; determination by NMR and MS fragmentation;
参考文献
Canadian Journal of Chemistry, , vol. 68, # 3 p. 492 - 501
反应条件
in tetrahydrofuran Irradiation (UV/VIS); (N2 or Ar); 250-W sun lamp, 3 h; colorless solution is filtered, (1)H-NMR;
参考文献
Canadian Journal of Chemistry, , vol. 68, # 3 p. 492 - 501
反应条件
1: ethyl 2-bromo-2-methyl propionate With indium in tetrahydrofuran 0.333333 h; Sonication; 2: formaldehyd in tetrahydrofuran 4 h; Sonication;
参考文献
Soengas, Raquel G.; Estevez, Amalia M.
Synlett, 2010 , # 17 p. 2625 - 2627
参考文献
Bischoff
Chemische Berichte, 1891 , vol. 24, p. 1053
反应条件
4-phenyl-acetophenone; zinc; benzene T=150°C; Reagens 4: Toluol;
参考文献
Bloom; Hauser
Journal of the American Chemical Society, 1944 , vol. 66, p. 153
反应条件
zinc in 1,4-dioxane; diethyl ether Substitution; 0.166667 h; Heating;
参考文献
Fotin; Shchepin; Vakhrin
Russian Journal of Organic Chemistry, 1999 , vol. 35, # 9 p. 1278 - 1281
