2,4-二甲基-3-戊醇合成路线 (共 83 条)
参考文献
Poletajew
Chemische Berichte, 1891 , vol. 24, p. 1309
反应条件
ammonium cerium (IV) nitrate; lithium bromide in water; acetonitrile T=65°C; 5 h;
参考文献
Nikishin; Sokova; Kapustina
Russian Chemical Bulletin, 2010 , vol. 59, # 2 p. 391 - 395
反应条件
cerium (III) nitrate hexahydrate; dihydrogen peroxide; lithium bromide in water; acetonitrile T=65 - 70°C; 6 h;
参考文献
Kapustina; Sokova; Nikishin
Russian Chemical Bulletin, 2010 , vol. 59, # 6 p. 1284 - 1288
反应条件
hydrogenchloride T=0 - 20°C;
参考文献
Whitmore; Johnston
Journal of the American Chemical Society, 1938 , vol. 60, p. 2266
反应条件
trichloroacetonitrile; triphenylphosphine in 1,2-dichloro-benzene T=-7°C; 24 h; other alcohols; other halogenating agents; also with use of iodide and thiocyanate ions; var. solvents, temp. and reaction times; Product distribution;
参考文献
Matveeva, E. D.; Yalovskaya, A. I.; Cherepanov, I. A.; Bundel', Yu. G.; Kurts, A. L.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, # 8.1 p. 1409 - 1415
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, # 8 p. 1611 - 1618
参考文献
Whitmore; Johnston
Journal of the American Chemical Society, 1938 , vol. 60, p. 2266
反应条件
1: 76 percent / xylene / 0.5 h / Heating 2: 88 percent / methane sulfonyl azide, Et3N / acetonitrile / 3 h / Ambient temperature 3: 78 percent / 8 percent KOH / acetonitrile / 14 h / Ambient temperature View Scheme
参考文献
Mueller, Paul; Polleux, Philippe
Helvetica Chimica Acta, 1994 , vol. 77, p. 645 - 654
参考文献
Poletajew
Chemische Berichte, 1891 , vol. 24, p. 1309
反应条件
potassium hydroxide; Ru(CF3CO2)CO(PPh3)2 T=140°C; 200 h; Equilibrium constant;
参考文献
Graser, Barbara; Strohmeier, Walter; Marcec, Radovan; Steigerwald, Hannelore
Berichte der Bunsen-Gesellschaft, 1981 , vol. 85, # 7 p. 671 - 677
反应条件
aluminum oxide
T=398°C;
参考文献
Henne; Matuszak
Journal of the American Chemical Society, 1944 , vol. 66, p. 1651
Full Text Show Details
Goldwasser; Taylor
Journal of the American Chemical Society, 1939 , vol. 61, p. 1757