4-乙酰基-N,N-二甲基苯磺酰胺合成路线 (共 6 条)
反应条件
bromine in 1,4-dioxane; diethyl ether
参考文献
Hassan, Saber M.; El-Maghraby, Ahmed A.; Abdel Aal, Mahmoud M.; Bashandy, Mahmoud S.
Phosphorus, Sulfur and Silicon and the Related Elements, 2009 , vol. 184, # 2 p. 291 - 308
参考文献
Beecham Group p.l.c.
Patent: US4812470 A1, 1989 ;
反应条件
in tetrahydrofuran; water
Yield given;
参考文献
De Vleeschauwer, Marc; Gauthier, Jacques Yves
Synlett, 1997 , vol. 1997, # 4 p. 375 - 377
反应条件
magnesium nitrate hexahydrate; potassium permanganate; acetone
参考文献
Du Pont de Nemours and Co.
Patent: US2680135 , 1952 ;
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Du Pont de Nemours and Co.
Patent: DE1013291 , 1957 ;
反应条件
2: KMnO4; aqueous acetone; Mg(NO3)2
View Scheme
参考文献
Du Pont de Nemours and Co.
Patent: US2680135 , 1952 ;
反应条件
(i) SO2, (diazotization), (ii) /BRN= 605257/, H2O; Multistep reaction;
参考文献
Leclerc,G. et al.
Journal of Medicinal Chemistry, 1977 , vol. 20, # 12 p. 1657 - 1662