1,2-二甲氧基-9,10-蒽醌合成路线 (共 37 条)
反应条件
silver(l) oxide in N,N-dimethyl-formamide
参考文献
Kuhn,R.; Trischmann,H.
Chemische Berichte, 1961 , vol. 94, p. 2258 - 2263
反应条件
barium dihydroxide in N,N-dimethyl-formamide
Heating;
参考文献
Kuhn,R.; Trischmann,H.
Chemische Berichte, 1961 , vol. 94, p. 2258 - 2263
反应条件
lithium diisopropyl amide
1.) THF, hexane, -78 deg C, 10 min, 2.) THF, hexane, from-40 deg C to RT, 2 h; Yield given. Multistep reaction;
参考文献
Khanapure; Reddy; Biehl
Journal of Organic Chemistry, 1987 , vol. 52, # 26 p. 5685-5690
参考文献
Etienne; Weill-Raynal
Bulletin de la Societe Chimique de France, 1953 , p. 1142,1144
参考文献
Savard, Jacques; Brassard, Paul
Tetrahedron, 1984 , vol. 40, # 18 p. 3455 - 3464
反应条件
chromium(VI) oxide; trifluoroacetic anhydride
1.) CH2Cl2, 0 deg C to rt, 2.) aq. AcOH, rt, 3 h; Yield given. Multistep reaction;
参考文献
Almeida, Wanda P.; Costa, Paulo R.R.
Synthetic Communications, 1996 , vol. 26, # 23 p. 4507 - 4518
参考文献
Weizmann; Bergmann
Journal of the Chemical Society, 1936 , p. 567
反应条件
1.) CH2Cl2, 0 deg C, 2.) Chromatographie an SiO2; Yield given. Multistep reaction;
参考文献
Gompper, Rudolf; Sramek, Maria
Synthesis, 1981 , # 8 p. 649 - 650
参考文献
Perkin,A.G.
Journal of the Chemical Society, 1907 , vol. 91, p. 2069
反应条件
1: concentrated sulfuric acid; nitrating mixture
2: potash
View Scheme
参考文献
Hoechster Farbw.
Patent: DE158278 ;