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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
60040-14-4
合成路线
（共 12 条）
60040-14-4
→
反应条件
69971-79-5
4-戊基-4’-碘联苯
反应条件
1: With sulfuric acid; sodium nitrite in water T=0 - 5°C; 2 h; 2: With urea in water T=0 - 5°C; 3: With potassium iodide in water Sandmeyer Reaction; 1 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 78, # 5 p. 1768 - 1777
121219-12-3
4-戊基苯硼酸
+
106-40-1
对溴苯胺
→
反应条件
7116-96-3
4-正戊基联苯
+
60040-14-4
反应条件
water; sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in ethylene glycol dimethyl ether 0.5 h; Heating;
参考文献
Hird, Michael; Seed, Alexander J.; Toyne, Kenneth J.
Synlett, 1999 , # 4 p. 438 - 440
121219-12-3
4-戊基苯硼酸
+
540-37-4
对碘苯胺
→
反应条件
7116-96-3
4-正戊基联苯
+
60040-14-4
反应条件
water; sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in ethylene glycol dimethyl ether 0.5 h; Heating;
参考文献
Hird, Michael; Seed, Alexander J.; Toyne, Kenneth J.
Synlett, 1999 , # 4 p. 438 - 440
1391953-45-9
→
反应条件
60040-14-4
反应条件
1: With hydrogenchloride; tin in ethanol; water 6 h; Reflux; 2: With sodium carbonate in water pH=9;
参考文献
Kobr, Lukas; Zhao, Ke; Shen, Yongqiang; Polivkova, Katerina; Shoemaker, Richard K.; Clark, Noel A.; Price, John C.; Rogers, Charles T.; Michl, Josef
Journal of Organic Chemistry, 2013 , vol. 78, # 5 p. 1768 - 1777
638-29-9
戊酰氯
→
反应条件
60040-14-4
反应条件
1: AlCl3 2: N2H4, KOH View Scheme
参考文献
Melamed; Nuckols; Fox
Tetrahedron Letters, 1994 , vol. 35, # 45 p. 8329 - 8332
92-52-4
联苯
→
反应条件
60040-14-4
反应条件
1: 68 percent / AlCl3 / CCl4 / Ambient temperature 2: 57 percent / H2SO4, KNO3 / 1 h / 0 °C 3: 1) hydrazine hydrate, 2) KOH / 1) diethylene glycol, 180 deg C, 2) reflux, overnight View Scheme
参考文献
Bailey, A. L.; Bates, Gordon S.
Molecular Crystals and Liquid Crystals (1969-1991), 1991 , vol. 198, p. 417 - 428
51554-95-1
对戊基溴苯
→
反应条件
60040-14-4
反应条件
1.1: n-butyllithium / tetrahydrofuran / 0.17 h / |Inert atmosphere; |Cooling with acetone-dry ice 1.2: -78 - 20 °C / |Inert atmosphere 1.3: 48 h / 20 °C / |Inert atmosphere 2.1: tin; hydrogenchloride / water; ethanol / 6 h / |Reflux 2.2: pH 9 View Scheme
参考文献
Kobr, Lukas; Zhao, Ke; Shen, Yongqiang; Polivkova, Katerina; Shoemaker, Richard K.; Clark, Noel A.; Price, John C.; Rogers, Charles T.; Michl, Josef
Journal of Organic Chemistry, 2013 , vol. 78, # 5 p. 1768 - 1777
636-98-6
4-硝基碘苯
→
反应条件
60040-14-4
反应条件
1.1: n-butyllithium / tetrahydrofuran / 0.17 h / |Inert atmosphere; |Cooling with acetone-dry ice 1.2: -78 - 20 °C / |Inert atmosphere 1.3: 48 h / 20 °C / |Inert atmosphere 2.1: tin; hydrogenchloride / water; ethanol / 6 h / |Reflux 2.2: pH 9 View Scheme
参考文献
Kobr, Lukas; Zhao, Ke; Shen, Yongqiang; Polivkova, Katerina; Shoemaker, Richard K.; Clark, Noel A.; Price, John C.; Rogers, Charles T.; Michl, Josef
Journal of Organic Chemistry, 2013 , vol. 78, # 5 p. 1768 - 1777
4075-79-0
4-乙酰氨基联苯
→
反应条件
60040-14-4
反应条件
1: AlCl3 2: N2H4, KOH View Scheme
参考文献
Melamed; Nuckols; Fox
Tetrahedron Letters, 1994 , vol. 35, # 45 p. 8329 - 8332
60040-09-7
→
反应条件
60040-14-4
反应条件
potassium hydroxide; hydrazine hydrate 1) diethylene glycol, 180 deg C, 2) reflux, overnight; Yield given. Multistep reaction;
参考文献
Bailey, A. L.; Bates, Gordon S.
Molecular Crystals and Liquid Crystals (1969-1991), 1991 , vol. 198, p. 417 - 428
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