2-甲基-1,3-二噻烷合成路线 （共 22 条）
反应条件
1: 1.) butyllithium / 1.) thf, hexane, 2.) thf, hexane, from -78 deg C to RT, overnight
2: 1.) trifluoroacetic anhydride, DMSO, 2.) triethylamine / 1.) dichloromethane, -78 deg C, 1 h, 2.) dichloromethane, from -78 deg C to RT, overnight
View Scheme
参考文献
Page, Philip C. Bulman; Wilkes, Robin D.; Namwindwa, Ernest S.; Witty, Michael J.
Tetrahedron, 1996 , vol. 52, # 6 p. 2125 - 2154
反应条件
1: 1.) butyllithium / 1.) thf, hexane, 2.) thf, hexane, from -78 deg C to RT, overnight
2: 1.) trifluoroacetic anhydride, DMSO, 2.) triethylamine / 1.) dichloromethane, -78 deg C, 1 h, 2.) dichloromethane, from -78 deg C to RT, overnight
View Scheme
参考文献
Page, Philip C. Bulman; Wilkes, Robin D.; Namwindwa, Ernest S.; Witty, Michael J.
Tetrahedron, 1996 , vol. 52, # 6 p. 2125 - 2154
