反应条件
1: 82 percent / Et3N / CH2Cl2 / 2 h / 0 °C
2: 70 percent / CuCl*tris(pyridin-2-ylmethyl)amine complex / 1,2-dichloro-ethane / 80 °C
3: 92 percent / Bu3SnH; AIBN / cyclohexane / 3 h / 80 °C
View Scheme
参考文献
De Campo, Floryan; Lastecoueres, Dominique; Verlhac, Jean-Baptiste
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 4 p. 575 - 580