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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
60084-12-0
合成路线
（共 20 条）
948040-42-4
+
70-23-5
3-溴丙酮酸乙酯
→
反应条件
948040-43-5
+
60084-12-0
反应条件
in ethanol T=80°C; Hantzsch reaction; 0.833333 h;
参考文献
Popsavin, Mirjana; Spaic, Sasa; Svircev, Milos; Kojic, Vesna; Bogdanovic, Gordana; Popsavin, Velimir
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 15 p. 4123 - 4127
1188366-53-1
→
反应条件
948040-43-5
+
60084-12-0
反应条件
trichloromonobromomethane; 1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane T=0 - 4°C; 77 h;
参考文献
Popsavin, Mirjana; Spaic, Sasa; Svircev, Milos; Kojic, Vesna; Bogdanovic, Gordana; Pejanovic, Vjera; Popsavin, Velimir
Tetrahedron, 2009 , vol. 65, # 36 p. 7637 - 7645
70-23-5
3-溴丙酮酸乙酯
+
615249-45-1
→
反应条件
60084-12-0
+
615249-46-2
反应条件
in ethanol T=80°C; Hantzsch reaction; 0.833333 h;
参考文献
Popsavin, Mirjana; Torovic, Ljilja; Kojic, Vesna; Bogdanovic, Gordana; Spaic, Sasa; Popsavin, Velimir
Bioorganic and Medicinal Chemistry Letters, 2003 , vol. 13, # 19 p. 3167 - 3170
23316-67-8
1-氰基-2,3,5-三苯甲酰氧基-β-D-呋喃核糖
→
反应条件
60084-12-0
反应条件
1: Et3N / methanol / 3 h / 20 °C 2: 85 percent / MnO2 / benzene / 12 h / Heating View Scheme
参考文献
Ramasamy, Kanda S.; Bandaru, Rajanikanth; Averett, Devron
Journal of Organic Chemistry, 2000 , vol. 65, # 18 p. 5849 - 5851
70-23-5
3-溴丙酮酸乙酯
+
781642-73-7
→
反应条件
60084-12-0
+
781642-75-9
反应条件
in ethanol 0.833333 h; Heating;
参考文献
Popsavin, Mirjana; Torovic, Ljilja; Kojic, Vesna; Bogdanovic, Gordana; Popsavin, Velimir
Tetrahedron Letters, 2004 , vol. 45, # 38 p. 7125 - 7128
948040-40-2
→
反应条件
60084-12-0
反应条件
1: mesyl chloride; pyridine / 2.5 h / -15 - 20 °C 2: 90 percent / hydrogen sulfide; pyridine / 4 h / 20 °C 3: 11 percent / ethanol / 0.83 h / 80 °C View Scheme
参考文献
Popsavin, Mirjana; Spaic, Sasa; Svircev, Milos; Kojic, Vesna; Bogdanovic, Gordana; Popsavin, Velimir
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 15 p. 4123 - 4127
948040-41-3
→
反应条件
60084-12-0
反应条件
1: 90 percent / hydrogen sulfide; pyridine / 4 h / 20 °C 2: 11 percent / ethanol / 0.83 h / 80 °C View Scheme
参考文献
Popsavin, Mirjana; Spaic, Sasa; Svircev, Milos; Kojic, Vesna; Bogdanovic, Gordana; Popsavin, Velimir
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 15 p. 4123 - 4127
157506-37-1
→
反应条件
60084-12-0
反应条件
1: TFA; hydrochloric acid / 140 h / 4 °C 2: hydroxylamine hydrochloride; NaOAc / ethanol; CH2Cl2 / 24 h / 20 °C 3: mesyl chloride; pyridine / 2.5 h / -15 - 20 °C 4: 90 percent / hydrogen sulfide; pyridine / 4 h / 20 °C 5: 11 percent / ethanol / 0.83 h / 80 °C View Scheme
参考文献
Popsavin, Mirjana; Spaic, Sasa; Svircev, Milos; Kojic, Vesna; Bogdanovic, Gordana; Popsavin, Velimir
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 15 p. 4123 - 4127
228399-09-5
→
反应条件
60084-12-0
反应条件
1: TFA; aq. HCl / 72 h / 4 °C 2: NH2OH*HCl; NaOAc / ethanol; CH2Cl2 / 2 h / 20 °C 3: MsCl; pyridine / 2.5 h / -15 - 20 °C 4: 34 percent / H2S; pyridine / 2 h / 20 °C 5: 67 percent / TiCl4 / CH2Cl2 / 1 h / 0 °C 6: 22 percent / ethanol / 0.83 h / Heating View Scheme
参考文献
Popsavin, Mirjana; Torovic, Ljilja; Kojic, Vesna; Bogdanovic, Gordana; Popsavin, Velimir
Tetrahedron Letters, 2004 , vol. 45, # 38 p. 7125 - 7128
781642-71-5
→
反应条件
60084-12-0
反应条件
1: 34 percent / H2S; pyridine / 2 h / 20 °C 2: 67 percent / TiCl4 / CH2Cl2 / 1 h / 0 °C 3: 22 percent / ethanol / 0.83 h / Heating View Scheme
参考文献
Popsavin, Mirjana; Torovic, Ljilja; Kojic, Vesna; Bogdanovic, Gordana; Popsavin, Velimir
Tetrahedron Letters, 2004 , vol. 45, # 38 p. 7125 - 7128
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