反应条件
1: 98 percent / imidazole / dimethylformamide / 1 h 2: 89 percent / 0.67 h / Heating 3: LAH / diethyl ether / 1 h 4: pyridinium chlorochromate (PCC) / CH2Cl2 / 6 h 5: HCl / diethyl ether / 0.75 h / 0 °C 6: TBAF / tetrahydrofuran / 22 h / Ambient temperature 7: 80 percent / ZnI2 / CHCl3 / 72 h / Ambient temperature 8: pyridine, DMAP / 22 h 9: NaBH4 / dimethylsulfoxide / 3 h / 85 °C 10: PhI(OOCCF3)2, H2O / ethanol / 0.17 h / Ambient temperature View Scheme
参考文献
Journal of the American Chemical Society, , vol. 114, # 1 p. 304 - 317
