N-苄基-2-溴-2-甲基丙酰胺合成路线 （共 31 条）
反应条件
in N,N-dimethyl-formamide
T=25°C; electroreduction; Rate constantEquilibrium constant;
参考文献
Maran, Flavio; Celadon, Dino; Severin, Maria Gabriella; Vianello, Elio
Journal of the American Chemical Society, 1991 , vol. 113, # 24 p. 9320 - 9329
参考文献
Quast,H. et al.
Liebigs Annalen der Chemie, 1979 , p. 74 - 82
反应条件
1: 1. NaH / 1. dioxane, 1h; 2. 100 deg C, 4h
2: 88 percent / NaH, 10percent N,N'-Dimethyl-N,N'-propyleneurea (DMPU) / dimethylformamide / 100 °C
View Scheme
参考文献
Coutts, Ian G. C.; Southcott, Mark R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , p. 767 - 771
反应条件
1: 34 percent / sodium hydride / benzene / 3 h / Heating
2: 92 percent / saturated aq. sodium hydrogen carbonate / CHCl3
View Scheme
参考文献
Zanotti, Giuseppe; Filira, Fernando; Pra, Antonio Del; Cavicchioni, Giorgio; Veronese, Augusto C.; D'Angeli, Ferruccio
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2249 - 2253
反应条件
sodium hydride
1.5 h;
参考文献
Scrimin, Paolo; D'Angeli, Feruccio; Veronese, Augusto C.; Baioni, Valentino
Tetrahedron Letters, 1983 , vol. 24, # 41 p. 4473 - 4476
反应条件
tetrabutylammomium bromide in acetonitrile
electrochemical reduction at -1.7 V; Yield given. Yields of byproduct given;
参考文献
Maran, Flavio; Vianello, Elio; D'Angeli, Ferruccio; Cavicchioni, Giorgio; Vecchiati, Giorgio
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1987 , p. 33 - 39
反应条件
N(Et)4ClO4; methyl iodide in N,N-dimethyl-formamide
T=15°C; mercury catode;
参考文献
Casadei, Maria Antonietta; Cesa, Stefania; Inesi, Achille; Moracci, Franco Micheletti
Journal of Chemical Research, Miniprint, 1995 , # 5 p. 1064 - 1079
反应条件
N(Et)4ClO4 in N,N-dimethyl-formamide
T=15°C; mercury catode;
参考文献
Casadei, Maria Antonietta; Cesa, Stefania; Inesi, Achille; Moracci, Franco Micheletti
Journal of Chemical Research, Miniprint, 1995 , # 5 p. 1064 - 1079
反应条件
tri-n-butyl-tin hydride; 2,2'-azo-bisisobutyronitrile in toluene
14 h; Heating;
参考文献
Nishio, Takehiko; Iseki, Kyoko; Araki, Norihito; Miyazaki, Takenori
Helvetica Chimica Acta, 2005 , vol. 88, # 1 p. 35 - 41
反应条件
N(Et)4ClO4 in acetonitrile
electrochemical reduction at -1.5 V; Yield given. Yields of byproduct given;
参考文献
Maran, Flavio; Vianello, Elio; Cavicchioni, Giorgio; D'Angeli, Ferruccio
Journal of the Chemical Society, Chemical Communications, 1985 , # 10 p. 660
