sodium hydroxide; 4-hydroxyacetophenone oxime-derived palladacycle in water T=120°C; 0.166667 h; microwave irradiation;

1: 3,3,5,5-tetramethyl-3,5-disila-4-oxa-1,6-heptadiene With methanol; sulfuric acid T=5 - 10°C; 1 h; 2: monomethyl trimethoxy silane T=5 - 10°C; 1.5 h; 3: With sulfuric acid; water more than 3 stages;

1: With methanol; sulfuric acid T=5 - 10°C; 0.75 h; 2: With water T=5 - 25°C; 3.5 h; Product distribution / selectivity;

1: tris(vinyldimethylsiloxy)methylsilane With tetrabutyl ammonium fluoride in tetrahydrofuran T=20°C; 0.166667 h; 2: 4'-iodoacetophenone With bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran T=20°C; 0.166667 h;