四(二甲基乙烯基硅氧基)硅烷合成路线 (共 2 条)
反应条件
1: 3,3,5,5-tetramethyl-3,5-disila-4-oxa-1,6-heptadiene With methanol; sulfuric acid T=5 - 10°C; 1 h; 2: orthosilicic acid tetramethyl ester T=5 - 10°C; 1.5 h; 3: With sulfuric acid; water more than 3 stages;
参考文献
Shin-Etsu Chemical Co., Ltd.
Patent: EP1510520 A1, 2005 ;
Location in patent: Page/Page column 15 ;
反应条件
pyridine; lithium orthosilicate; sodium carbonate 0.5 h;
参考文献
Kalmychkov, G. V.; Yarosch, N. K.; Mirskov, R. G.; Voronkov, M. G.; Rakhlin, V. I.
J. Gen. Chem. USSR (Engl. Transl.), 1992 , vol. 62, # 3.2 p. 710 - 711,590