9-(4-溴苯基)-3,6-二-叔丁基-9h-咔唑合成路线 （共 4 条）
反应条件
1: With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 4 h; 2: With 1-iodo-tridecafluoro-hexane in tetrahydrofuran; hexane T=-78 - 20°C;
参考文献
Wang, Changsheng; Batsanov, Andrei S.; West, Kara; Bryce, Martin R.
Organic Letters, 2008 , vol. 10, # 14 p. 3069 - 3072
反应条件
copper(l) iodide; potassium carbonate; L-proline in dimethyl sulfoxide
T=140°C; Ullmann reaction; Inert atmosphere;
参考文献
Lai, Wen-Yong; He, Qi-Yuan; Chen, Dao-Yong; Huang, Wei
Chemistry Letters, 2008 , vol. 37, # 9 p. 986 - 987
反应条件
1: 94 percent / ZnCl2 / nitromethane / 5 h / 20 °C
2: 82 percent / K2CO3; Cu; 18-crown-6 / 1,2-dichloro-benzene / 12 h / Heating
View Scheme
参考文献
Liu, Yu; Nishiura, Masayoshi; Wang, Yue; Hou, Zhaomin
Journal of the American Chemical Society, 2006 , vol. 128, # 17 p. 5592 - 5593
反应条件
copper(l) iodide; potassium carbonate in 1,2-dichloro-benzene
Inert atmosphere;
参考文献
Deng, Lijun; Li, Jiuyan; Wang, Xinzeng; Zhang, Zhengchuan
Journal of Materials Chemistry, 2012 , vol. 22, # 37 p. 19700 - 19708,9
Title/Abstract Full Text Show Details
Deng, Lijun; Wang, Xinzeng; Zhang, Zhengchuan; Li, Jiuyan
Journal of Materials Chemistry, 2012 , vol. 22, # 37 p. 19700 - 19708
