1: palladium 10 on activated carbon / water; ethyl acetate / 0.17 h / 25 °C / 2828.7 Torr / |Inert atmosphere 2: sodium hydroxide / ethanol / 1.5 h / 78 °C / |Inert atmosphere 3: hydrogenchloride / isopropanol acetate / 2.67 h / 20 - 25 °C View Scheme
参考文献
Prashad, Mahavir; Hu, Bin; Har, Denis; Repic, Oljan; Blacklock, Thomas J.; Lohse, Olivier
Organic Process Research and Development, 2006 , vol. 10, # 1 p. 135 - 141
1: palladium 10 on activated carbon / water; ethyl acetate / 0.17 h / 25 °C / 2828.7 Torr / |Inert atmosphere 2: sodium hydroxide / ethanol / 1.5 h / 78 °C / |Inert atmosphere View Scheme
参考文献
Prashad, Mahavir; Hu, Bin; Har, Denis; Repic, Oljan; Blacklock, Thomas J.; Lohse, Olivier
Organic Process Research and Development, 2006 , vol. 10, # 1 p. 135 - 141
1.1: AlCl3, aluminium chloride / neat (no solvent) / 0.25 h / 0 - 5 °C
1.2: 255 / 1 h / 0 - 10 °C
2.1: hydrogen; 5 palladium on charcoal / ethanol; water / 25 °C / 2250.23 Torr / |Inert atmosphere
3.1: AlCl3, aluminium chloride / dichloromethane / 0.75 h / 0 °C
3.2: 1 h / 0 - 5 °C
View Scheme
参考文献
Prashad, Mahavir; Hu, Bin; Har, Denis; Repic, Oljan; Blacklock, Thomas J.; Lohse, Olivier
Organic Process Research and Development, 2006 , vol. 10, # 1 p. 135 - 141
1.1: hydrogen; 5 palladium on charcoal / ethanol; water / 25 °C / 2250.23 Torr / |Inert atmosphere
2.1: AlCl3, aluminium chloride / dichloromethane / 0.75 h / 0 °C
2.2: 1 h / 0 - 5 °C
View Scheme
参考文献
Prashad, Mahavir; Hu, Bin; Har, Denis; Repic, Oljan; Blacklock, Thomas J.; Lohse, Olivier
Organic Process Research and Development, 2006 , vol. 10, # 1 p. 135 - 141
1.1: isopropanol acetate / 3.17 h / 0 - 25 °C
2.1: AlCl3, aluminium chloride / neat (no solvent) / 0.25 h / 0 - 5 °C
2.2: 255 / 1 h / 0 - 10 °C
3.1: hydrogen; 5 palladium on charcoal / ethanol; water / 25 °C / 2250.23 Torr / |Inert atmosphere
4.1: AlCl3, aluminium chloride / dichloromethane / 0.75 h / 0 °C
4.2: 1 h / 0 - 5 °C
View Scheme
参考文献
Prashad, Mahavir; Hu, Bin; Har, Denis; Repic, Oljan; Blacklock, Thomas J.; Lohse, Olivier
Organic Process Research and Development, 2006 , vol. 10, # 1 p. 135 - 141
palladium 10 on activated carbon in water; ethyl acetate
T=25°C; P=2828.7 Torr; 0.166667 h; Inert atmosphere; SolventReagent/catalyst;
参考文献
Prashad, Mahavir; Hu, Bin; Har, Denis; Repic, Oljan; Blacklock, Thomas J.; Lohse, Olivier
Organic Process Research and Development, 2006 , vol. 10, # 1 p. 135 - 141