in tetrahydrofuran
T=-10°C; 2.66 h; Inert atmosphereFlow reactor;
参考文献
Murray, Philip R. D.; Browne, Duncan L.; Pastre, Julio C.; Butters, Chris; Guthrie, Duncan; Ley, Steven V.
Organic Process Research and Development, 2013 , vol. 17, # 9 p. 1192 - 1208
1: With diphenyl-N,N-bis-((S,S)-1-naphthalen-2-yl-ethyl)phosphinamine; copper(ll) bromide in diethyl ether
T=-30°C; 3 h;
2: With ammonium chloride in diethyl ether; water
optical yield given as percent eeenantioselective reaction;
