(1R,4S)-顺-4-乙酰氧基-2-环戊烯-1-醇合成路线 （共 32 条）
反应条件
Pancreatin; triethylamine in tetrahydrofuran T=20°C; 3 h;
参考文献
Synlett, , # 3 p. 485 - 487
反应条件
sodium hydroxide; phosphate buffer; immobilized porcine liver esterase (PLE, E. C. 3.1.1.1) on Eupergit C T=32°C; 14 h; pH= 7;
参考文献
Tetrahedron Letters, , vol. 26, # 4 p. 407 - 410
反应条件
triethylamine in tetrahydrofuran 4 h; Ambient temperaturelipase from Mucor sp.;
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. 333, # 3 p. 497 - 499
反应条件
lipase EC 3.1.1.3 L10 in water; acetone T=5 - 25°C; 6.5 h; Product distribution / selectivity;
参考文献
US2008/39635 A1, ;
Page/Page column 4-5 ;
反应条件
tetrabutyl ammonium fluoride; triethylamine in tetrahydrofuran
参考文献
Tetrahedron Asymmetry, , vol. 7, # 10 p. 2791 - 2792
反应条件
T=50°C; acrylic supported Candida antarctica lipase B;
参考文献
Journal of the American Chemical Society, , vol. 115, # 23 p. 11014 - 11015
反应条件
1: 53 percent / KH2PO4, H3PO4 / H2O / 40 h / 99 °C / pH 4.1 2: 76 percent / PPTs / tetrahydrofuran / 18 h / Ambient temperature 3: LiAlH4, LiI / various solvent(s); toluene / 0.5 h / -20 - -13 °C 4: 45 percent / Et3N, pancreatin, vinyl acetate / various solvent(s) / 7 h / Ambient temperature 5: p-TsOH / ethanol / 2 h / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 53, # 6 p. 1983 - 2004
反应条件
1: 76 percent / PPTs / tetrahydrofuran / 18 h / Ambient temperature 2: LiAlH4, LiI / various solvent(s); toluene / 0.5 h / -20 - -13 °C 3: 45 percent / Et3N, pancreatin, vinyl acetate / various solvent(s) / 7 h / Ambient temperature 4: p-TsOH / ethanol / 2 h / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 53, # 6 p. 1983 - 2004
反应条件
Pancreatin; triethylamine in tetrahydrofuran T=20°C; Enzymatic reaction;
参考文献
Organic Process Research and Development, , vol. 2, # 6 p. 357 - 365
