8-氨基-3-beta-D-呋喃核糖基咪唑并[4,5-g]喹唑啉合成路线 （共 3 条）
反应条件
1.1: methanol; water / 0.33 h / 20 °C
1.2: 20 °C
2.1: N,O-bis-(trimethylsilyl)-acetamide / acetonitrile / 0.33 h / Inert atmosphere; Reflux
2.2: 2.5 h / Inert atmosphere; Reflux
3.1: methanol; ammonia / 36 h / 100 °C / Inert atmosphere
View Scheme
参考文献
Hernandez, Armando R.; Kool, Eric T.
Organic Letters, 2011 , vol. 13, # 4 p. 676 - 679
反应条件
1.1: N,O-bis-(trimethylsilyl)-acetamide / acetonitrile / 0.33 h / Inert atmosphere; Reflux
1.2: 2.5 h / Inert atmosphere; Reflux
2.1: methanol; ammonia / 36 h / 100 °C / Inert atmosphere
View Scheme
参考文献
Hernandez, Armando R.; Kool, Eric T.
Organic Letters, 2011 , vol. 13, # 4 p. 676 - 679
反应条件
1.1: N,O-bis-(trimethylsilyl)-acetamide / acetonitrile / 0.33 h / Inert atmosphere; Reflux
1.2: 2.5 h / Inert atmosphere; Reflux
2.1: methanol; ammonia / 36 h / 100 °C / Inert atmosphere
View Scheme
参考文献
Hernandez, Armando R.; Kool, Eric T.
Organic Letters, 2011 , vol. 13, # 4 p. 676 - 679
