3-羟基-2-硝基苯甲酸合成路线 （共 44 条）
反应条件
1: KMnO4, aq. NaOH 2: Py*HCl / 180 - 190 °C View Scheme
参考文献
Australian Journal of Chemistry, , vol. 29, p. 2003 - 2021
参考文献
Chemische Berichte, , vol. 11, p. 1734
Chemische Berichte, , vol. 20, p. 407
反应条件
1: water 2: KOH-solution View Scheme
参考文献
Chemische Berichte, , vol. 11, p. 1734
Chemische Berichte, , vol. 20, p. 407
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 43, p. 464
参考文献
Chemische Berichte, , vol. 11, p. 1734
Chemische Berichte, , vol. 20, p. 407
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 40, p. 624
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 178, p. 1286
Chemische Berichte, , vol. 20, p. 408
参考文献
Journal of the Chemical Society, , vol. 119, p. 1425
Recueil des Travaux Chimiques des Pays-Bas, , vol. 40, p. 623
反应条件
copper in 1-methyl-pyrrolidin-2-one T=250°C; 0.5 h;
参考文献
Zhang, Yun; Jamison, Timothy F.; Patel, Sejal; Mainolfi, Nello
Organic Letters, 2011 , vol. 13, # 2 p. 280 - 283
反应条件
1: methanol With thionyl chloride T=0°C; 0.5 h; 2: 3-Hydroxy-2-nitro-benzoic acid 4 h; Heating / reflux;
参考文献
PFIZER PRODUCTS INC.
Patent: WO2007/125405 A2, 2007 ;
Location in patent: Page/Page column 24; 72-73 ;
WO 2007/125405 A2
反应条件
1: methanol With thionyl chloride T=0°C; 0.5 h; 2: 3-Hydroxy-2-nitro-benzoic acid 6 h; Reflux;
参考文献
Gavai, Ashvinikumar V.; DeLucca, George V.; O'Malley, Daniel; Gill, Patrice; Quesnelle, Claude A.; Fink, Brian E.; Zhao, Yufen; Lee, Francis Y.
Patent: US2014/87992 A1, 2014 ;
Location in patent: Paragraph 0314-0315 ;
