1,1'-联-2-萘酚 合成路线 （共 233 条）
反应条件
pyridine; trichlorophosphate T=20°C; phosphorylation; 1 h;
参考文献
Chen, Chun Xia; Xu, Rong; Li, Bin
→
反应条件
198573-86-3 [(1R)-[1,1'-联萘]-2,2'-二醇][(1R)-[1,1'-联苯]-2,2'-二基二[(1,2,3,4,5-H)-3,4-二甲基-2,4-环戊二烯-1-亚基]]-钛
反应条件
in toluene inert atmosphere; addn. of soln. of binaphthyl to soln. of Ti-complex, stirring (4 d, 100°C); evapn., dissol. in pentane, filtration (Celite); elem. anal.;
参考文献
Ringwald, Markus; Stuermer, Rainer; Brintzinger, Hans H.
反应条件
1.1: NaH / tetrahydrofuran / 0 - 20 °C 1.2: 100 percent / tetrahydrofuran / 4.5 h / 20 °C 2.1: n-BuLi / diethyl ether; hexane / 3 h / 20 °C 2.2: 85 percent / dibromotetrachloroethane / diethyl ether; hexane; tetrahydrofuran / 0.25 h / 20 °C View Scheme
参考文献
Lv, Na; Xie, Meilan; Gu, Weibing; Ruan, Huanyang; Qiu, Song; Zhou, Chunshan; Cui, Zheng
反应条件
in toluene heating for 36 h;
参考文献
Reetz, Manfred T.; Gosberg, Andreas; Goddard, Richard; Kyung, Suk-Hun
→
反应条件
198491-04-2 [(1R)-[1,1'-联萘]-2,2'-二醇][(1R)-[1,1'-联苯]-2,2'-二基二[(1,2,3,4,5-H)-3,4-二甲基-2,4-环戊二烯-1-亚基]]-锆
反应条件
in dichloromethane inert atmosphere; addn. of binaphthol to soln. of Zr-complex; mixt. of stereoisomers not sepd.;
参考文献
Ringwald, Markus; Stuermer, Rainer; Brintzinger, Hans H.
反应条件
potassium carbonate; sodium iodide in acetone Heating;
参考文献
Dong, Chune; Zhang, Junlong; Zheng, Weizhong; Zhang, Liangfu; Yu, Zuolong; Choi, Michael C.K.; Chan, Albert S.C.
反应条件
sodium hydroxide; tetrabutylammomium bromide in water; toluene T=20 - 50°C; 6.33333 h; Product distribution / selectivity;
参考文献
Wang, Licai; Gao, Zhanxian; Li, Wei; Zheng, Guotong; Dong, Qingxin; Liu, Riping; Wang, Xiaohuan; Zhang, Nan; Wang, Jingzhuang; Cai, Shimian
反应条件
ammonium chloride in benzene 12 h; Heating;
参考文献
Hulst; De Vries; Feringa
反应条件
1.1: 11 percent / triphenylphosphine; Br2 / acetonitrile / 230 - 300 °C 2.1: t-BuLi / pentane; tetrahydrofuran / 0.25 h / -78 °C 2.2: 80 percent / aq. NH4Cl / tetrahydrofuran; pentane / -78 - 20 °C View Scheme
参考文献
Clayden, Jonathan; Kubinski, Przemyslaw M.; Sammiceli, Federica; Helliwell, Madeleine; Diorazio, Louis
反应条件
in acetonitrile T=80°C; 1.5 h;
参考文献
Maslennikova, Vera I.; Merkulov, Roman V.; Dyagileva, Maria V.; Vasyanina, Larisa K.; Lyssenko, Konstantin A.; Antipin, Mikhail Yu.; Weber, Dirk; Bauer, Ingmar; Habicher, Wolf D.; Nifantyev, Eduard E.
