1,1'-联-2-萘酚合成路线 （共 233 条）
反应条件
pyridine; trichlorophosphate T=20°C; phosphorylation; 1 h;
参考文献
Chen, Chun Xia; Xu, Rong; Li, Bin
Science China Chemistry, 2012 , vol. 55, # 7 p. 1257 - 1262
反应条件
bei der trocknen Destillation;
参考文献
Dianin
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1874 , vol. 6, p. 183
Chemische Berichte, 1873 , vol. 6, p. 1252
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Walder
Chemische Berichte, 1882 , vol. 15, p. 2170
反应条件
pyridine; trichlorophosphate T=20°C; phosphorylation; 1 h;
参考文献
Chen, Chun Xia; Xu, Rong; Li, Bin
Science China Chemistry, 2012 , vol. 55, # 7 p. 1257 - 1262
反应条件
zinc beim Destillieren;
参考文献
Walder
Chemische Berichte, 1882 , vol. 15, p. 2170
反应条件
1: 100 percent / pyridine / CH2Cl2 / 6 h / 0 °C 2: 95 percent / diisopropylethylamine / palladium diacetate, 1,4-bis(diphenylphosphino)butane / dimethylsulfoxide / 12 h / 100 °C 3: 81 percent / NiCl2(dppe) / diethyl ether / 24 h / Heating 4: 79 percent / NEt3, Cl3SiH / xylene / 3 h / 120 °C View Scheme
参考文献
Uozumi, Yasuhiro; Tanahashi, Asako; Lee, Sang-Yong; Hayashi, Tamio
Journal of Organic Chemistry, 1993 , vol. 58, # 7 p. 1945 - 1948
反应条件
1: 100 percent / pyridine / CH2Cl2 / 6 h / 0 °C 2: 95 percent / diisopropylethylamine / palladium diacetate, 1,4-bis(diphenylphosphino)butane / dimethylsulfoxide / 12 h / 100 °C 3: 81 percent / NiCl2(dppe) / diethyl ether / 24 h / Heating View Scheme
参考文献
Uozumi, Yasuhiro; Tanahashi, Asako; Lee, Sang-Yong; Hayashi, Tamio
Journal of Organic Chemistry, 1993 , vol. 58, # 7 p. 1945 - 1948
反应条件
1: 100 percent / pyridine / CH2Cl2 / 6 h / 0 °C 2: 95 percent / diisopropylethylamine / palladium diacetate, 1,4-bis(diphenylphosphino)butane / dimethylsulfoxide / 12 h / 100 °C 3: 81 percent / NiCl2(dppe) / diethyl ether / 24 h / Heating 4: 79 percent / NEt3, Cl3SiH / xylene / 3 h / 120 °C View Scheme
参考文献
Uozumi, Yasuhiro; Tanahashi, Asako; Lee, Sang-Yong; Hayashi, Tamio
Journal of Organic Chemistry, 1993 , vol. 58, # 7 p. 1945 - 1948
反应条件
zeolite HSZ-360 in neat (no solvent) T=60°C; 12 h;
参考文献
Tetrahedron Letters, , vol. 39, # 33 p. 6049 - 6052
反应条件
aluminium trichloride in nitrobenzene T=25°C; 8 h;
参考文献
Synthesis, , # 24 p. 3821 - 3826
反应条件
4-(N,N-dimethlyamino)pyridine in isopropyl alcohol T=20°C;
参考文献
Organic Process Research and Development, , vol. 11, # 5 p. 870 - 876
