1,1'-联-2-萘酚合成路线 （共 233 条）
反应条件
1: pyridine; 4-(N,N-dimethlyamino)pyridine / toluene; dichloromethane / 6 h / 0 - 20 °C 2: Arthrobacter sp. lipase / dimethyl sulfoxide; aq. phosphate buffer / 24 h / 25 °C / pH 7 / |Resolution of racemate; |Enzymatic reaction View Scheme
参考文献
Gupta, Pankaj; Rouf, Abdul; Shah, Bhahwal Ali; Mahajan, Neha; Chaubey, Asha; Taneja, Subhash Chandra
Journal of Molecular Catalysis B: Enzymatic, 2014 , vol. 101, p. 35 - 39
反应条件
in acetonitrile racemate resolution; 4 h; Heating;
参考文献
Wang, Yang; Sun, Jie; Ding, Kuiling
Tetrahedron, 2000 , vol. 56, # 26 p. 4447 - 4451
反应条件
1.1: bromine / dichloromethane / 2 h / -78 °C / |Inert atmosphere 2.1: sodium hydride / mineral oil; tetrahydrofuran / 1 h / 0 °C / |Inert atmosphere 2.2: 4.5 h / 0 - 20 °C / |Inert atmosphere View Scheme
参考文献
Lv, Na; Xie, Meilan; Gu, Weibing; Ruan, Huanyang; Qiu, Song; Zhou, Chunshan; Cui, Zheng
Organic Letters, 2013 , vol. 15, # 10 p. 2382 - 2385
反应条件
potassium hydroxide; N,N-dimethylthiocarbamoyl chloride
Yield given. Multistep reaction;
参考文献
Bandarage, Upul K.; Simpson, Jim; Smith, Robin A. J.; Weavers, Rex T.
Tetrahedron, 1994 , vol. 50, # 11 p. 3463 - 3472
反应条件
zeolite HSZ-360 in various solvent(s)
5 h; Heating;
参考文献
Arienti, Attilio; Bigi, Franca; Maggi, Raimondo; Moggi, Pietro; Rastelli, Massimo; Sartori, Giovanni; Trere, Alessandra
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 9 p. 1391 - 1393
参考文献
Brass; Patzelt
Chemische Berichte, 1937 , vol. 70, p. 1341,1343, 1347
Full Text Show Details
Ioffe
Zhurnal Obshchei Khimii, 1933 , vol. 3, p. 437,441
Chem. Zentralbl., 1935 , vol. 106, # I p. 392
反应条件
T=200 - 220°C; Destillieren des Reaktionsprodukts;
参考文献
Marschalk
Bulletin de la Societe Chimique de France, 1928 , vol. <4> 43, p. 1394
Full Text Show Details
Corbellini; Aymar
Giorn. Chim. ind. appl., vol. 10, p. 198
Full Text Show Details
Comp. nat. Mat. col.
Patent: DE469553 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 16, p. 1392
参考文献
Corbellini; Aymar
Giorn. Chim. ind. appl., vol. 10, p. 196
Chem. Zentralbl., 1928 , vol. 99, # II p. 146
Full Text Show Details
Hansgirg
Patent: DE386040 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 14, p. 479
反应条件
bei der Destillation;
参考文献
Marschalk
Bulletin de la Societe Chimique de France, 1928 , vol. <4> 43, p. 1394
Full Text Show Details
Corbellini; Aymar
Giorn. Chim. ind. appl., vol. 10, p. 198
Full Text Show Details
Comp. nat. Mat. color.
Patent: DE469553 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 16, p. 1392
反应条件
1: 45 percent / Ph3PBr2 / 320 °C
2: 1) t-BuLi / 1) THF, -90 deg C
3: 21 percent / TiCl3, Zn/Cu / Heating
View Scheme
参考文献
Dubois, Fabien; Gingras, Marc
Tetrahedron Letters, 1998 , vol. 39, # 28 p. 5039 - 5040
