1,1'-联-2-萘酚合成路线 (共 233 条)
反应条件
triethylamine in acetonitrile T=30°C; 1 h; Inert atmosphereIrradiation;
参考文献
Journal of Organic Chemistry, , vol. 75, # 10 p. 3477 - 3480
反应条件
boron tribromide in dichloromethane T=0 - 20°C;
参考文献
Tetrahedron Asymmetry, , vol. 9, # 20 p. 3607 - 3610
反应条件
1: (S)-6,6'-dibromo-2,2'-dihydroxy-1,1'-binaphthyl With n-butyllithium in tetrahydrofuran; hexane T=-78 - -70°C; 5 h; Inert atmosphere; 2: carbonic acid dimethyl ester in tetrahydrofuran; hexane T=-78 - -40°C; 1.5 h; Inert atmosphere; 3: With hydrogenchloride in tetrahydrofuran; hexane; water T=20°C; pH=< 1; Cooling with ice;
参考文献
Journal of Organic Chemistry, , vol. 76, # 7 p. 2319 - 2323
反应条件
tert-butylamine; copper dichloride in methanol T=23°C; 24 h; Yield given;
参考文献
Tetrahedron Letters, , vol. 31, # 3 p. 413 - 416
反应条件
1: methanol; acetone / Ambient temperature 2: aq. FeCl3*6H2O / 5 h / 55 °C View Scheme
参考文献
Chemical Communications, , # 7 p. 693 - 694
反应条件
oxygen; copper(l) chloride in methanol 0.333333 h; Ambient temperature; Yields of byproduct given;
参考文献
Duchstein, Hans-Juergen; Mueller, Klaus; Wurm, Gotthard
Archiv der Pharmazie (Weinheim, Germany), 1988 , vol. 321, p. 153 - 157
反应条件
2-aminonaphthalene-3-carboxylic acid methyl ester; tert-butylamine in methanol 48 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 59, # 8 p. 2156 - 2163
反应条件
1: Boc-[(R)-Binol-22-C-6]-(R)-Bip-OMe With boron tribromide in dichloromethane T=-10 - 20°C; 48 h; 2: methanol With thionyl chloride T=20°C; 168 h;
参考文献
Tetrahedron Letters, , vol. 44, # 9 p. 1741 - 1745
反应条件
ammonium cerium(IV) nitrate 0.0833333 h; microwave irradiation;
参考文献
Journal of Chemical Research, , # 11 p. 733 - 735
反应条件
triethylamine in isopropyl alcohol T=30°C; 1 h; Inert atmosphereIrradiation;
参考文献
Verga, Daniela; Doria, Filippo; Pretali, Luca; Freccero, Mauro
Journal of Organic Chemistry, 2010 , vol. 75, # 10 p. 3477 - 3480