2,3,4,5,6-五氟苯甲酸合成路线 (共 133 条)
反应条件
in tetrahydrofuran reaction at 20°C, 3 hours;;
参考文献
Gmelin Handbook: F: PerFHalOrg.4, 2.2.4, page 68 - 115
反应条件
formic acid; dihydrogen peroxide 5 h;
参考文献
Furin,G.G.; Miller,A.O.
Journal of Fluorine Chemistry, 1985 , vol. 28, p. 23
反应条件
dihydrogen peroxide in dichloromethane 10 h;
参考文献
Journal of Fluorine Chemistry, , vol. 28, p. 23
反应条件
1: 85 percent / pyridine / diethyl ether / 1.5 h / Heating 2: 80 percent / H2 / 5 percent Pd/C / methanol / 760 Torr / Ambient temperature 3: 5 percent / potassium carbonate / H2O / 10 h / Heating View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 54, # 11 p. 3447 - 3452
反应条件
1: 80 percent / H2 / 5 percent Pd/C / methanol / 760 Torr / Ambient temperature 2: 5 percent / potassium carbonate / H2O / 10 h / Heating View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 54, # 11 p. 3447 - 3452
反应条件
in various solvent(s) T=20°C; Oxidation;
参考文献
Journal of Physical Organic Chemistry, , vol. 12, # 9 p. 688 - 694
反应条件
1: nitrogen; iron / 500 °C 2: H2SO4 View Scheme
参考文献
Nature (London, United Kingdom), , vol. 183, p. 588
反应条件
in tetrahydrofuran 0.5 hours;;
参考文献
Gmelin Handbook: F: PerFHalOrg.4, 2.2.4, page 68 - 115
反应条件
ammonium cerium(IV) nitrate; 1-ethyl-3-methylimidazolium trifluoromethanesulfonate T=125°C; 8 h;
参考文献
Journal of Organic Chemistry, , vol. 72, # 2 p. 517 - 524