2,3,4,5,6-五氟苯甲酸合成路线 (共 133 条)
反应条件
NiCl2*3Bpy; [N-butylthiazolium][Br]; zinc in water T=70°C; 7 h;
参考文献
Prikhod'ko, Sergey A.; Adonin, Nicolay Yu.; Parmon, Valentin N.
Tetrahedron Letters, 2010 , vol. 51, # 17 p. 2265 - 2268
反应条件
air; Titanium(IV) oxide T=25°C; 1 h; Photolysis;
参考文献
Ravichandran; Selvam; Muruganandham; Swaminathan
Journal of Fluorine Chemistry, 2006 , vol. 127, # 9 p. 1204 - 1210
反应条件
dicyclohexyl-carbodiimide in toluene Ambient temperature;
参考文献
Weintraub, Susan T.; Satsangi, Rajiv K.; Simmons, Anne Marie; Williams, Robert F.; Neal Pinckard
Analytical Chemistry, 1993 , vol. 65, # 17 p. 2400 - 2402
反应条件
[Fe(II)(TPA)(CH3CN)2](OTf)2; water; dihydrogen peroxide in acetonitrile T=20°C;
参考文献
Das, Parthapratim; Que Jr., Lawrence
Inorganic Chemistry, 2010 , vol. 49, # 20 p. 9479 - 9485
反应条件
Ag2CO3; oxygen; palladium diacetate in dimethyl sulfoxide T=130°C; Sealed tube;
参考文献
Luo, Hai-Qing; Dong, Wen; Loh, Teck-Peng
Tetrahedron Letters, 2013 , vol. 54, # 22 p. 2833 - 2836
反应条件
silver carbonate; bis[2-(diphenylphosphino)phenyl] ether; palladium dichloride in dimethyl sulfoxide T=150°C; 1 h;
参考文献
Becht, Jean-Michel; Le Drian, Claude
Organic Letters, 2008 , vol. 10, # 14 p. 3161 - 3164
反应条件
[N-butylthiazolium][Br]; zinc in water T=70°C; 7 h;
参考文献
Tetrahedron Letters, , vol. 51, # 17 p. 2265 - 2268
反应条件
NiCl2*3Bpy; [N-butylthiazolium][Br]; zinc in water T=70°C; 7 h;
参考文献
Tetrahedron Letters, , vol. 51, # 17 p. 2265 - 2268
反应条件
1: SiCl4 / benzene / Heating 2: 275 °C / 740 Torr View Scheme
参考文献
Sartori,P.; Weidenbruch,M.
Chemische Berichte, 1967 , vol. 100, p. 3016 - 3023
反应条件
thionyl chloride 2 h; Reflux;
参考文献
Chen, Yin-Bo; Li, Ji-Ling; Shao, Xu-Sheng; Xu, Xiao-Yong; Li, Zhong
Chinese Chemical Letters, 2013 , vol. 24, # 8 p. 673 - 676