4-氯-4'-碘-1,1'-联苯合成路线 （共 13 条）
反应条件
T=131°C; thermolysis; Product distributionMechanism;
参考文献
Mackay, Donald; McIntyre, Deane Douglas
Canadian Journal of Chemistry, 1982 , vol. 60, p. 990 - 999
反应条件
potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in 1,4-dioxane
T=100°C; 3 h;
参考文献
SMITHKLINE BEECHAM CORPORATION
Patent: WO2007/71434 A1, 2007 ;
Location in patent: Page/Page column 34-35 ;
反应条件
1: 4-(4-chlorophenyl)iodobenzene With n-butyllithium in diethyl ether; hexane
T=-78°C; Inert atmosphere;
2: With boric acid trimethyl ester in diethyl ether; hexane
T=-78 - 20°C;
3: 2,3-dimethylbutane-2,3-diol Further stages;
参考文献
Wallmann, Ivonne; Schnakenburg, Gregor; Luetzen, Arne
Synthesis, 2009 , # 1 p. 79 - 84
