(6-甲氧基萘-2-基)甲醇合成路线 （共 23 条）
反应条件
1: With n-hexylMgCl; FeBr2; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=20°C; 0.0833333 h; Inert atmosphere; 2: in di-isopropyl ether; toluene T=120°C; 24 h; Inert atmosphere; Reagent/catalystSolvent;
参考文献
Yu, Da-Gang; Wang, Xin; Zhu, Ru-Yi; Luo, Shuang; Zhang, Xiao-Bo; Wang, Bi-Qin; Wang, Lei; Shi, Zhang-Jie
Journal of the American Chemical Society, 2012 , vol. 134, # 36 p. 14638 - 14641
反应条件
1: ZnCl2, SOCl2 / dioxane / 0.67 h 2: acetonitrile; H2O / 19 h / Heating View Scheme
参考文献
McCarthy, James R.; Huffman, John C.
Journal of Organic Chemistry, 1984 , vol. 49, # 25 p. 4995 - 4997
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in water; acetic acid 4 h; Heating;
参考文献
Tetrahedron, , vol. 58, # 26 p. 5251 - 5265
反应条件
1: gaseous HCl / benzene / 2 h / 60 °C 2: dimethylformamide / 3 h / Ambient temperature 3: 64.1 percent / cc. H2SO4 / methanol / 6 h / Heating View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 30, # 2 p. 428 - 439
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
T=20°C; 8 h;
参考文献
Shi, Zhen-Dan; Yang, Bing-Hui; Zhao, Jing-Jing; Wu, Yu-Lin; Ji, Yong-Yong; Yeh, Ming
Bioorganic and Medicinal Chemistry, 2002 , vol. 10, # 7 p. 2171 - 2175
反应条件
lithium aluminium tetrahydride
参考文献
Mukerjee, Y. N.; Gaur, S. P.; Jain, P. C.; Anand, Nitya
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 985 - 987
反应条件
sodium bis(2-methoxyethoxy)aluminium dihydride in diethyl ether
参考文献
Haydock; Mulholland; Telford; et al.
European Journal of Medicinal Chemistry, 1984 , vol. 19, # 3 p. 205 - 214
反应条件
sodium tetrahydroborate in methanol
T=20°C; 1 h;
参考文献
Matsunaga, Nobuyuki; Kaku, Tomohiro; Ojida, Akio; Tanaka, Toshimasa; Hara, Takahito; Yamaoka, Masuo; Kusaka, Masami; Tasaka, Akihiro
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 16 p. 4313 - 4336
反应条件
lithium aluminium tetrahydride in diethyl ether
1 h; Ambient temperature;
参考文献
Itoh; Miyake; Tanabe; Hirata; Oka
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 6 p. 2006 - 2015
参考文献
Imperial Chemical Industries Limited
Patent: US4107329 A1, 1978 ;
Title/Abstract Full Text Show Details
Imperial Chemical Industries Limited
Patent: US4055595 A1, 1977 ;
