反应条件
1: trimethyl-oxo-sulfonium iodide With sodium hydride in N,N-dimethyl-formamide; mineral oil
1 h; Inert atmosphere;
2: With copper(l) iodide in N,N-dimethyl-formamide; mineral oil
0.5 h; Inert atmosphere;
3: β-methyl-β-nitrostyrene in N,N-dimethyl-formamide; mineral oil
T=0 - 20°C; 2.33333 h; Inert atmosphere;
参考文献
Mikhaylov, Andrey A.; Dilman, Alexander D.; Struchkova, Marina I.; Khomutova, Yulia A.; Korlyukov, Alexander A.; Ioffe, Sema L.; Tartakovsky, Vladimir A.
Tetrahedron, 2011 , vol. 67, # 25 p. 4584 - 4594