1,4,7,10-四氮杂环十二烷-1,4,7,10-四乙酸合成路线 (共 13 条)
反应条件
1: potassium carbonate / chloroform / 52 h / 20 °C 2: trifluoroacetic acid / dichloromethane / 12 h View Scheme
参考文献
Chemical Communications, , vol. 49, # 6 p. 564 - 566
反应条件
in water pH=7; 1 h; Kinetics; Further Variations:pH-values;
参考文献
Journal of Labelled Compounds and Radiopharmaceuticals, , vol. 44, p. S814 - S816
反应条件
in water addn. of gadolinium oxide to aq. soln. of tetraazacyclododecane deriv., mixt. heated at 90°C for 12 h; cooling to room temp., addn. of cation-exchange and anion-exchange resins, stirring for 60 min at room temp., filtration, filtrate freeze dried;
参考文献
Oliver, Morag; Ahmad, Ayesha; Kamaly, Nazila; Perouzel, Eric; Caussin, Annabelle; Keller, Michael; Herlihy, Amy; Bell, Jimmy; Miller, Andrew D.; Jorgensen, Michael R.
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 18 p. 3489 - 3497