1,3-二(羟基甲基)-1,3-二氢-2H-苯并咪唑-2-硫酮合成路线 (共 7 条)
反应条件
T=150 - 195°C; other N-hydroxymethylbenzimidaazoles; ΔH; Thermodynamic data;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 34, # 7 p. 677 - 678
反应条件
1: SOCl2 2: LiAlH4; diethyl ether View Scheme
参考文献
Zinner et al.
Chemische Berichte, 1957 , vol. 90, p. 2852,2854
反应条件
in ethanol; water
hydroxymethylation; 0.166667 h; Heatingultrasound irradiation;
参考文献
Zhong; Song; Peng; Qian
Synthetic Communications, 2000 , vol. 30, # 20 p. 3801 - 3807
参考文献
Zinner et al.
Chemische Berichte, 1957 , vol. 90, p. 2852,2854
反应条件
1: aqueous methanol
2: acetic acid
View Scheme
参考文献
Zinner et al.
Chemische Berichte, 1957 , vol. 90, p. 2852,2854
反应条件
Erwaermen des Reaktionsprodukts mit CS2;
参考文献
Donau-Pharmazie G.m.b.H.
Patent: DE1021370 , 1952 ;
参考文献
Zinner et al.
Chemische Berichte, 1957 , vol. 90, p. 2852,2854