反应条件
in diethyl ether byproducts: O2; addn. a soln. of benzoyl peroxide in ether to a suspn. of Ni(PPh3)3 in ether at -50°C, stirring for 1 h at 22°C, (Ar); filtn. of ppt. (Ni(OCOPh)2*H2O), washing (benzene, ether), drying in vacuum at 110°C, evapn. of mother soln., addn. of MeOH, filtn. of ppt. (Ni(CO)(PPh3)3, drying in vacuum, evapn. of MeOH, recrystn. of residue (PPh3) from ethanol;
参考文献
Inorganica Chimica Acta, , vol. 171, p. 29 - 34
