in dichloromethane
1 equiv of PPh3, CH2Cl2, 23°C; not sepd., detected by UV spectra;
参考文献
Mandimutsira, Beaven S.; Ramdhanie, Bobby; Todd, Ryan C.; Wang, Hailin; Zareba, Adelajda A.; Czernuszewicz, Roman S.; Goldberg, David P.
Journal of the American Chemical Society, 2002 , vol. 124, # 51 p. 15170 - 15171
→
反应条件
in acetone
react. (Cu2(μ-O)2(Me2-tpa)2)(PF6)2 with PPh3 in acetone at -78°C under Ar atm.;
参考文献
Hayashi, Hideki; Fujinami, Shuhei; Nagatomo, Shigenori; Ogo, Seiji; Suzuki, Masatatsu; Uehara, Akira; Watanabe, Yoshihito; Kitagawa, Teizo
Journal of the American Chemical Society, 2000 , vol. 122, # 9 p. 2124 - 2125
tetrachloromethane; triethylamine in dichloromethane
T=50 - 60°C;
参考文献
Stolzenberg, Heribert; Weinberger, Bernd; Fehlhammer, Wolf Peter; Puehlhofer, Frank G.; Weiss, Robert
European Journal of Inorganic Chemistry, 2005 , # 21 p. 4263 - 4271
Balema, Viktor P.; Wiench, Jerzy W.; Pruski, Marek; Pecharsky, Vitalij K.
Journal of the American Chemical Society, 2002 , vol. 124, # 22 p. 6244 - 6245
in dichloromethane
slow addn. of PPh3 to the peroxo-dicopper(II) complex; elem. anal.;
参考文献
Sanyal, Indrajit; Strange, Richard W.; Blackburn, Ninian J.; Karlin, Kenneth D.
Journal of the American Chemical Society, 1991 , vol. 113, # 12 p. 4692 - 4693
