反应条件
in toluene
react. performed under an atmosphere of pure dinitrogen, mixt. of Mo2O3{S2P(OMe)2}4 (2.0 mmol) and Ph3P (0.525 g, 2.0 mmol) refluxed in toluene (50 ml) for 1h, addn. of K{HB(Me2pz)3} (1.48 g, 4.4 mmol) to cooled mixt., refluxed for 4h;; filtration in air, solvent removed in vacuo, column chromatography (SiO2/CH2Cl2), recrystn. from CH2Cl2; elem. anal.;;
参考文献
Roberts, Sue A.; Young, Charles G.; Cleland, W. E. Jr.; Ortega, Richard B.; Enemark, John H.
Inorganic Chemistry, 1988 , vol. 27, p. 3044 - 3051
